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1 article(s) from Hammond, Marcus J

The development and evaluation of a continuous flow process for the lipase- mediated oxidation of alkenes

Charlotte Wiles,
Marcus J. Hammond and
Paul Watts

Beilstein J. Org. Chem. 2009, 5, No. 27, doi:10.3762/bjoc.5.27

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Graphical Abstract

Scheme 1: Illustration of the chemo-enzymatic epoxidation of an alkene; involving the biocatalytic perhydroly...

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Scheme 2: Illustration of the chemo-enzymatic epoxidation of 1-methylcyclohexene (6) to 1-methylcyclohexene o...

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Scheme 3: Model reaction used to compare the continuous flow epoxidation strategy with the conventional batch...

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Figure 1: Schematic of the reaction set-up used to evaluate the continuous flow chemo-enzymatic epoxidation o...

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Figure 2: Graph illustrating the effect of flow rate (hence residence time) on the conversion of 1-methylcycl...

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Figure 3: Graph illustrating the effect of (a) flow rate and (b) residence time on the conversion of 1-methyl...

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Figure 4: Graph illustrating the effect of oxidant stoichiometry on the conversion of 1-methylcyclohexene (6)...

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Figure 5: Illustration of the enzyme 4 stability to H₂O₂ (2) for the conversion of 1-methylcyclohexene (6) to...

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Scheme 4: Illustration of the reaction products obtained when conducting the continuous flow epoxidation of c...

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Published 02 Jun 2009

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